This paper presents a new technology of surface treatment of the grid made of molybdenum plate by electric spark machining. Procedures of the new technology are as follows: a. Boiling in 10% NaOH solution; b. Ultrasonic treating with emery + HCl solution; c. Ultrasonic treating with emery+Fe+++ Sal+H2O+small inhibitor; d. Electro-polishing with H3PO4-H2SO4-C3H5(OH)3-H2O solution.