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一种Sc2O3掺杂Y-Gd-Hf-O压制式直热式阴极发射特性研究

王兴起 王小霞 罗积润 漆世锴 李云

王兴起, 王小霞, 罗积润, 漆世锴, 李云. 一种Sc2O3掺杂Y-Gd-Hf-O压制式直热式阴极发射特性研究[J]. 电子与信息学报, 2022, 44(4): 1382-1387. doi: 10.11999/JEIT210111
引用本文: 王兴起, 王小霞, 罗积润, 漆世锴, 李云. 一种Sc2O3掺杂Y-Gd-Hf-O压制式直热式阴极发射特性研究[J]. 电子与信息学报, 2022, 44(4): 1382-1387. doi: 10.11999/JEIT210111
WANG Xingqi, WANG Xiaoxia, LUO Jirun, QI Shikai, LI Yun. Investigation on Thermionic Emission Characteristics of Pressed Sc2O3 Doped Y-Gd-Hf-O Directly-heated Cathode[J]. Journal of Electronics & Information Technology, 2022, 44(4): 1382-1387. doi: 10.11999/JEIT210111
Citation: WANG Xingqi, WANG Xiaoxia, LUO Jirun, QI Shikai, LI Yun. Investigation on Thermionic Emission Characteristics of Pressed Sc2O3 Doped Y-Gd-Hf-O Directly-heated Cathode[J]. Journal of Electronics & Information Technology, 2022, 44(4): 1382-1387. doi: 10.11999/JEIT210111

一种Sc2O3掺杂Y-Gd-Hf-O压制式直热式阴极发射特性研究

doi: 10.11999/JEIT210111
基金项目: 国家自然科学基金(61771454)
详细信息
    作者简介:

    王兴起:男,1993年生,博士生,研究方向为阴极电子学、新型热阴极电子发射材料

    王小霞:女,1976年生,研究员,研究方向为阴极电子学理论与技术、真空电子器件新型功能材料的开发与研制

    罗积润:男,1957年生,研究员,研究方向为大功率速调管、行波管和回旋管放大器的研制、微波毫米波材料的加工、微波能量的应用

    漆世锴:男,1987年生,博士,研究方向为阴极电子学

    李云:男,1986年生,高级工程师,研究方向为氧化物阴极的研制

    通讯作者:

    王兴起 15650703108@163.com

  • 中图分类号: O462.1

Investigation on Thermionic Emission Characteristics of Pressed Sc2O3 Doped Y-Gd-Hf-O Directly-heated Cathode

Funds: The National Natural Science Foundation of China (61771454)
  • 摘要: 为了提高Y-Gd-Hf-O阴极耐电子轰击能力,该文通过高能球磨、压制和高温氢气烧结,制备了一种Sc2O3掺杂Y-Gd-Hf-O压制式直热式阴极。该阴极在1550 °C工作温度下,经过10 W电子连续轰击480 h后,发射电流密度下降至初始值的87.5%,表现出良好的耐电子轰击能力。阴极表面的微观形貌、成分组成分析表明,经压制后氢气气氛烧结,阴极表面呈陶瓷状结构形态,有利于提高阴极的耐电子轰击能力;经高温烧结、激活后表面形成了n型半导体Y2O3-x层,对改善阴极表面导电性、降低逸出功和提高热发射有促进作用。
  • 图  1  Y-Gd-Hf-O压制式直热式阴极示意图

    图  2  阴极热发射测试二极管结构示意图

    图  3  阴极发射活性物XRD图

    图  4  阴极预处理前后表面微观形貌SEM

    图  5  阴极热发射性能曲线

    图  6  Richard 曲线

    图  7  阴极耐电子轰击测试曲线

    表  1  阴极氢炉烧结前后EDS原子含量(%)

    元素烧结前烧结后
    区域A区域B区域A区域B
    Y24.0824.3923.2323.99
    Gd3.222.942.962.95
    Hf14.5114.4614.8015.38
    Sc5.085.075.445.36
    O53.1153.1353.5752.32
    下载: 导出CSV
  • [1] ZHANG Xiaoke, HUA Yazhou, WANG Jinshu, et al. Studies of the influence of ZrH2 addition to the impregnant on the performance of yttrium oxide–tungsten matrix Ba dispenser cathodes[J]. IEEE Transactions on Electron Devices, 2021, 68(2): 829–834. doi: 10.1109/TED.2020.3045385
    [2] WANG Xiaoxia, WANG Xingqi, ZHAO Qinglan, et al. Research progress in new types of thermionic cathodes[C]. 13th IVESC, Bad Honnef, Germany, 2020: 18.
    [3] ROQUAIS J M and WIERSCHKE D J. Oxide cathode for electron gun with a differentially doped metallic substrate[P]. USA Patent, 522115, 2006.
    [4] GALLAGHER H E and KNAUER W. Thermionic emission cathode having reduced frontal area and enlarged emission area for ion bombardment environment[P]. USA Patent, 3439210DA, 1969.
    [5] KIRKWOOD D M, GROSS S J, BALK T J, et al. Frontiers in thermionic cathode research[J]. IEEE Transactions on Electron Devices, 2018, 65(6): 2061–2071. doi: 10.1109/TED.2018.2804484
    [6] 毕建明. W-Y2O3金属陶瓷阴极的二次发射[J]. 电子与信息学报, 1982, 4(2): 132–136.

    BI Jianming. Some secondary emission properties of W-Y2O3 cermet cathode[J]. Journal of Electronics &Information Technology, 1982, 4(2): 132–136.
    [7] 朱程, 杨金生, 李会成, 等. 30 kW连续波磁控管的研制[J]. 真空电子技术, 2013(5): 110–111. doi: 10.3969/j.issn.1002-8935.2013.05.030

    ZHU Cheng, YANG Jinsheng, LI Huicheng, et al. Development of 30 kW continuous wave magnetron[J]. Vacuum Electronics, 2013(5): 110–111. doi: 10.3969/j.issn.1002-8935.2013.05.030
    [8] 孙陵斌. 2 kW连续波磁控管阴极寿命的研究[J]. 真空电子技术, 2020(2): 51–53. doi: 10.16540/j.cnki.cn11-2485/tn.2020.02.12

    SUN Lingbin. Study on cathode lifetime of a 2 kW continuous wave magnetron[J]. Vacuum Electronics, 2020(2): 51–53. doi: 10.16540/j.cnki.cn11-2485/tn.2020.02.12
    [9] WANG Jinshu, ZHOU Meiling, MA Shuyun, et al. A study on the anti-electron-bombing life of La2O3–Y2O3–Mo cermet cathode materials[J]. Journal of Alloys and Compounds, 2006, 419(1/2): 172–175. doi: 10.1016/j.jallcom.2005.06.086
    [10] 漆世锴, 王小霞, 罗积润, 等. Y2O3-Gd2O3-HfO2掺杂W基直热式阴极的热发射及耐电子轰击特性[J]. 稀有金属材料与工程, 2018, 47(12): 3784–3788.

    QI Shikai, WANG Xiaoxia, LUO Jirun, et al. Thermionic emission and anti-electron-bombing characteristics of the Y2O3-Gd2O3-HfO2 doped W base direct-heated cathode[J]. Rare Metal Materials and Engineering, 2018, 47(12): 3784–3788.
    [11] 蒋鹏宇, 王小霞, 罗积润, 等. Y2O3-Gd2O3-HfO2浸渍W基直热式阴极次级电子发射的测试[J]. 微波学报, 2017, 33(S1): 250–253.

    JIANG Pengyu, WANG Xiaoxia, LUO Jirun, et al. Secondary electron emission of Y2O3-Gd2O3-HfO2 impregnated W base directly-heated cathode[J]. Journal of Microwaves, 2017, 33(S1): 250–253.
    [12] 陈晓倩, 王小霞, 张兆传, 等. Sc2O3掺杂对Y2O3-Gd2O3-HfO2难熔稀土氧化物直热式阴极热发射性能的影响[J]. 真空科学与技术学报, 2019, 39(2): 131–135. doi: 10.13922/j.cnki.cjovst.2019.02.07

    CHEN Xiaoqian, WANG Xiaoxia, ZHANG Zhaochuan, et al. Effect of Sc2O3-doping on thermal emission properties of Y2O3-Gd2O3-HfO2 thermal cathode[J]. Chinese Journal of Vacuum Science and Technology, 2019, 39(2): 131–135. doi: 10.13922/j.cnki.cjovst.2019.02.07
    [13] 郭艳群, 聂祚仁, 席晓丽, 等. 钨热电子发射材料的研究进展[J]. 稀有金属, 2005, 29(2): 200–205. doi: 10.3969/j.issn.0258-7076.2005.02.016

    GUO Yanqun, NIE Zuoren, XI Xiaoli, et al. Advances in research on tungsten cathode materials[J]. Chinese Journal of Rare Metals, 2005, 29(2): 200–205. doi: 10.3969/j.issn.0258-7076.2005.02.016
    [14] 漆世锴, 王小霞, 王兴起, 等. 大功率磁控管用新型Y2Hf2O7陶瓷阴极研究[J]. 物理学报, 2020, 69(3): 037901. doi: 10.7498/aps.69.20191496

    QI Shikai, WANG Xiaoxia, WANG Xingqi, et al. A novel Y2Hf2O7 ceramic cathode applied to high power magnetron tube[J]. Acta Physica Sinica, 2020, 69(3): 037901. doi: 10.7498/aps.69.20191496
    [15] CUI Yuntao, WANG Jinshu, LIU Wei, et al. Effect of Scandia on tungsten oxide powder reduction process[J]. Journal of Rare Earths, 2010, 28(S1): 202–205. doi: 10.1016/S1002-0721(10)60274-8
    [16] 赖陈, 王金淑, 周帆, 等. 新型钨铼混合基阴极的热电子发射性能[J]. 稀有金属材料与工程, 2016, 45(7): 1871–1875.

    LAI Chen, WANG Jinshu, ZHOU Fan, et al. Thermal electron emission properties of novel W-Re mixed matrix cathodes[J]. Rare Metal Materials and Engineering, 2016, 45(7): 1871–1875.
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出版历程
  • 收稿日期:  2021-02-01
  • 修回日期:  2021-07-01
  • 网络出版日期:  2021-08-24
  • 刊出日期:  2022-04-18

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