Advanced Search
Volume 43 Issue 9
Sep.  2021
Turn off MathJax
Article Contents
Fen LI, Guojian WANG, Hong TIAN, Yongliang LIU, Yanchun YU, Wei LÜ, Yanwen LIU. Evaporation Characteristics of Oxygen Free Copper for Microwave Vacuum Electron Devices[J]. Journal of Electronics & Information Technology, 2021, 43(9): 2751-2756. doi: 10.11999/JEIT200846
Citation: Fen LI, Guojian WANG, Hong TIAN, Yongliang LIU, Yanchun YU, Wei LÜ, Yanwen LIU. Evaporation Characteristics of Oxygen Free Copper for Microwave Vacuum Electron Devices[J]. Journal of Electronics & Information Technology, 2021, 43(9): 2751-2756. doi: 10.11999/JEIT200846

Evaporation Characteristics of Oxygen Free Copper for Microwave Vacuum Electron Devices

doi: 10.11999/JEIT200846
Funds:  The National Natural Science Foundation of China(61771454)
  • Received Date: 2020-09-30
  • Rev Recd Date: 2021-03-24
  • Available Online: 2021-04-15
  • Publish Date: 2021-09-16
  • As one of the commonly used materials for microwave vacuum electronic devices, the evaporation characteristics of oxygen free copper materials will affect the electrical properties of microwave vacuum electronic devices. In this paper, the effect of treatment process on the evaporation performance of oxygen free copper is studied by using ultra-high vacuum testing equipment. The thickness of evaporated copper film is measured by X-ray thickness gauge. And the surface morphology of oxygen free copper is observed by Scanning Electron Microscope (SEM). The results show that the macro-appearance surface roughness has little effect on the evaporation performance of oxygen free copper materials, but the treatment process has a great influence on the evaporation performance. The evaporation capacity of oxygen free copper will be increased after acid pickling and the evaporation capacity of oxygen free copper materials can be reduced by calcination in hydrogen. The evaporation capacity of oxygen free copper treated by deoiling cleaning and calcination in hydrogen is very low. The surface of oxygen free copper is analyzed. It is found that the vacuum evaporation performance of oxygen free copper material is related to the surface morphology of the material. The microscopic surface is smooth without oxidation and holes, and the vacuum evaporation of oxygen free copper material is less.
  • loading
  • [1]
    LIU Yanwen, TIAN Hong, LU Yuxin, et al. Influences of diamond material on heat dissipation capabilities of helical slow wave structures[J]. IEEE Transactions on Electron Devices, 2019, 66(12): 5321–5326. doi: 10.1109/TED.2019.2945969
    [2]
    LIU Yanwen, TIAN Hong, HAN Yong, et al. Temperature variation of a thermionic cathode during electron emission[J]. Science in China Series E: Technological Sciences, 2008, 51(9): 1497–1501. doi: 10.1007/s11431-008-0161-2
    [3]
    刘燕文, 王小霞, 田宏, 等. 纳米粒子薄膜热电子发射性能[J]. 中国科学: 信息科学, 2015, 45(1): 145–156. doi: 10.1360/N112013-00201

    LIU Yanwen, WANG Xiaoxia, TIAN Hong, et al. Study on emission properties of the nanopatical films[J]. Scientia Sinica Informationis, 2015, 45(1): 145–156. doi: 10.1360/N112013-00201
    [4]
    SHIN Y M, BARNETT L R, GAMZINA D, et al. Terahertz vacuum electronic circuits fabricated by UV lithographic molding and deep reactive ion etching[J]. Applied Physics Letter, 2009, 95(18): 181505. doi: 10.1063/1.3259823
    [5]
    刘燕文, 田宏, 陆玉新, 等. 用于浸渍阴极的钨海绵基体的净化[J]. 真空科学与技术学报, 2018, 38(2): 144–149. doi: 10.13922/j.cnki.cjovst.2018.02.12

    LIU Yanwen, TIAN Hong, LU Yuxin, et al. Purificationand cleaning of spongy tungsten disc used as impregnated dispenser-cathode in vacuum[J]. Chinese Journal of Vacuum Science and Technology, 2018, 38(2): 144–149. doi: 10.13922/j.cnki.cjovst.2018.02.12
    [6]
    DAYTON J A, MEARINI G T, CHEN H, et al. Diamond-studded helical traveling wave tube[J]. IEEE Transactions on Electron Devices, 2005, 52(5): 695–701. doi: 10.1109/TED.2005.845863
    [7]
    SENGELE S, JIANG Hongrui, BOOSKE J H, et al. Microfabrication and characterization of a selectively metallized W-band meander-line TWT circuit[J]. IEEE Transactions on Electron Devices, 2009, 56(5): 730–737. doi: 10.1109/TED.2009.2015416
    [8]
    刘燕文, 田宏, 韩勇, 等. 支取发射电流过程对热阴极温度影响的研究[J]. 中国科学E辑: 技术科学, 2008, 38(9): 1515–1520.

    LIU Yanwen, TIAN Hong, HAN Yong, et al. Study on the influence of discharge current on hot cathode temperature[J]. China Science E, 2008, 38(9): 1515–1520.
    [9]
    WANG Jinshu, ZHANG Xizhu, LIU Wei, et al. High current density Sc2O3-W matrix dispenser cathode[J]. Science China Information Sciences, 2012, 55(1): 98–105. doi: 10.1007/s11432-011-4518-y
    [10]
    WANG Xiaoxia, LIAO Xianheng, LUO Jirun, et al. Study on the Ni-Re-Ir sponge oxide cathode[J]. IEEE Transactions on Electron Devices, 2012, 59(2): 492–495.
    [11]
    刘燕文, 田宏, 韩勇, 等. 新型的覆纳米粒子薄膜阴极的研究[J]. 物理学报, 2009, 58(12): 8635–8642. doi: 10.3321/j.issn:1000-3290.2009.12.081

    LIU Yanwen, TIAN Hong, HAN Yong, et al. Emission properties of impregnated cathode with nanoparticle films[J]. Acta Physica Sinica, 2009, 58(12): 8635–8642. doi: 10.3321/j.issn:1000-3290.2009.12.081
    [12]
    LI Ji, YU Zhiqiang, SHAO Wensheng, et al. High current density M-type cathodes for vacuum electron devices[J]. Applied Surface Science, 2005, 251(1/4): 151–158.
    [13]
    WANG Xiaoxia, LIAO Xianheng, LUO Qinglan, et al. Performance of an oxide cathode prepared from submicrometer carbonates[J]. IEEE Transactions on Electron Devices, 2011, 58(9): 3195–3199. doi: 10.1109/TED.2011.2158648
    [14]
    电子工业生产技术手册编委会. 电子工业生产技术手册(4)[M]. 北京: 国防工业出版社, 1990: 317.

    Editorial Board of Production Technical Manual for Electronic Industry. Technical Manual for Electronic Industry (4)[M]. Beijing: National Defense Industry Press, 1990: 317.
    [15]
    刘燕文, 田宏, 韩勇, 等. 利用飞行时间质谱研究热阴极蒸发特性[J]. 真空科学与技术学报, 2007, 27(5): 437–441. doi: 10.3969/j.issn.1672-7126.2007.05.017

    LIU Yanwen, TIAN Hong, HAN Yong, et al. Time of flight mass spectroscopy study of thermonic cathode evaporation[J]. Chinese Journal of Vacuum Science and Technology, 2007, 27(5): 437–441. doi: 10.3969/j.issn.1672-7126.2007.05.017
    [16]
    刘燕文, 王小霞, 陆玉新, 等. 用于电真空器件的金属材料蒸发特性[J]. 物理学报, 2016, 65(6): 068502. doi: 10.7498/aps.65.068502

    LIU Yanwen, WANG Xiaoxia, LU Yuxin, et al. Study on evaporation from alloys used in microwave vacuum electron devices[J]. Acta Physica Sinica, 2016, 65(6): 068502. doi: 10.7498/aps.65.068502
    [17]
    周安林, 刘建伟, 李建峰, 等. 超导材料用无氧铜表面洁净化清洗工艺研究[J]. 低温物理学报, 2010, 32(2): 91–95.

    ZHOU Anlin, LIU Jianwei, LI Jianfeng, et al. Cleaning progress research of the oxygen-free copperfor superconducting materials[J]. Chinese Journal of Low Temperature Physics, 2010, 32(2): 91–95.
    [18]
    周安林, 陈江, 刘建伟, 等. 超导材料用无氧铜过硫酸钠溶液清洗工艺研究[J]. 低温物理学报, 2013, 35(4): 282–287.

    ZHOU Anlin, CHEN Jiang, LIU Jianfei, et al. Sodium persulfate solution cleaning progress research of the oxygen-free copper for superconducting materials[J]. Chinese Journal of Low Temperature Physics, 2013, 35(4): 282–287.
    [19]
    周安林. 无氧铜表面特定清洗液的腐蚀机制及溶液特性[J]. 表面技术, 2017, 46(1): 229–233. doi: 10.16490/j.cnki.issn.1001-3660.2017.01.037

    ZHOU Anlin. Corrosion mechanism and solution properties of specific cleaning solution for oxygen-free copper surface[J]. Surface Technology, 2017, 46(1): 229–233. doi: 10.16490/j.cnki.issn.1001-3660.2017.01.037
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(8)  / Tables(1)

    Article Metrics

    Article views (771) PDF downloads(43) Cited by()
    Proportional views
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return